IEC 62321-10-2020 pdf free
IEC 62321-10-2020 pdf free.Determination of certain substances in electrotechnical products – Part 10: Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS).
These test methods have been evaluated for use with plastics and rubbers. These test methods have been evaluated for use with ABS (acrylonitrile butadiene styrene) containing individual PAHs ranging from 37.2 mglkg to 119 mg/kg and rubbers containing individual PAHs ranging from 1 mg/kg to 221,2 mg/kg.
WARNING — This document does not purport to address all of the safety concerns, if any. associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
This horizontal standard is primarily intended for use by technical committees in the preparation of standards in accordance with the principles laid down in IEC Guide 108.
One of the responsibilities of a technical committee is, wherever applicable, to make use of horizontal standards in the preparation of its publications. The contents of this horizontal standard will not apply unless specifically referred to or included in the relevant publications.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
IEC 62321-1:2013, Determination of certain substances in electrotechnical products — Part 1:
Introduction and overview
IEC 6232 1-2, Determination of certain substances in electrotechnical products — Part 2:
Disassembly, disjointment and mechanical sample preparation
ISO 3696, Water for analytical laboratory use — Specification and test methods
3.1 Terms and definitions
No terms and definitions are listed in this document.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
• IEC Electropedia: available at http://www.electropedia.org/
• ISO Online browsing platform: available at http://www.iso.org/obp
3.2 Abbreviated terms
ABS acrylonitrile butadiene styrene
CCC continuing calibration check standard
El electron ionization
GC-MS gas chromatography-mass spectrometry
IS internal standard
IUPAC International Union of Pure and Applied Chemistry
LOD limit of detection
LOQ limit of quantificabon
MDL method detection limit
PAH polycyclic aromatic hydrocarbon
PBDE polybrominated diphenyl ether
QC quality control
RSD relative standard deviation
SIM selected ion monitoring
TICS tentatively identified compounds
US EPA United States Environmental Protection Agency
4 Principle
PAH compounds are quantitatively determined using ultrasonic extraction or Soxhlet extraction followed by gas chromatography-mass spectrometry (GC-MS) using single (or seIected) ion monitoring (SIM),
5 Reagents and materials
Use, as far as available, reagents of analytical quality, or better. Use only reagents with negligibly low concentrations of PAH and verify by blank determinations and, if necessary, apply additional cleaning steps (for calibrants, see 8.4):
a) Dichloromethane (GC grade or higher).
b) Helium (purity of greater than a volume fraction of 99,999 %).
c) Silica gel (purity of greater than a mass fraction of 99 %).
d) Toluene (GC grade or higher). IEC 62321-10 pdf free download.
